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Two Zone IR-Heating RTP Tube Furnace (4'' ID ) with Sliding Sample Holders - OTF-1200X-IR-IISL

Two Zone IR-Heating RTP Tube Furnace (4'' ID ) with Sliding Sample Holders - OTF-1200X-IR-IISL

Minimum Order: $20 (equipment), $100 (crystals)

Price: RFQ

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OTF-1200X-IR-IISL is a dual-zone IR heated rapid thermal processing (RTP) tube furnace with 4" ID quartz tube and two sliding sample holders for easy operation. It is capable of achieving a maximum heating rate of 50 °C/s and a cooling rate of 117 °C/min. The furnace is designed for growing two-dimension and superconducting materials via hybrid physical-chemical vapor deposition (HPCVD), where one heating zone is used as a solid evaporating source and another zone is for vapor deposition. The precision temperature controllers are able to set up programmable heating and cooling profiles with up to 30 temperature segments. 
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SPECIFICATIONS

Furnace Features
(optional)
  • Double-layer steel casing with air cooling keeps furnace surface temperature lower than 60°C.
  • Heated by shortwave IR tube lamps for fast heating
  • Two heating zones, 195 mm each, a total of 390 mm in length for HPCVD
  • Two sliding sample holders for easy loading/retrieving samples or fast cooling under ambient conditions. 
  • A retractable bellow is an option for the flange assembly, which allows flash heating and fast cooling under inert environment (optional).
  • Vacuum flanges and the digital vacuum gauge are installed for immediate use.
Power
  • AC 208-240V, single-phase, 50/60 Hz
  • MAX 24 kW, 100 A power supply required. (Max. peak experimental current: 78 A).
Heating Element
  • 16 pcs 1.5 kW halogen heating tubes, ( OD = 13.3 mm, L= 390 mm )
  • Standard working life: 2000 hrs. ( depends on the heating rate )
  • The halogen light tube is consumable. Please click the picture left to order spare.
Max. Temperature
  • 900°C max (< 10 minutes )
  • 800°C (< 30 minutes )
  • 600°C (continuous operation)
Temperature Accuracy
  • ± 1°C
Max. Heating Rate
  • RT ~ 800ºC: 50 ºC/s
  • 800 ºC ~ 900 ºC: 10 ºC/s
Max. Cooling Rate
  • 60 ºC/min under 200 mTorr environment
  • 117 ºC/min under atmospheric pressure
  • 10 °C/min slowest
Process Tube Size
  • High purity fused quartz tube
  • Φ110 (OD) × Φ106 (ID)× 740 (L) mm
Sliding Rails 
  • Dual sliding rails made of Cr plated steel
  • Sliding rail length: 400 mm
Thermocouple
  • Two K type, 1/4" Dia x 24" length

Temperature Controller

  • Two temperature controllers for controlling two zones independently via SCR
  • PID automatic control with up to 30 programmable segments for precise control of heating rate, cooling rate and dwell time.
  • Built-in thermocouple broken protection.
  • Over-temperature protection and alarm allow for operation without attendant(s).
  • ± 1 ºC temperature accuracy for dwelling.
  • RS485 Communications Port.
  • PC Control:
    • An MTS-02 control module is included for PC control on this furnace.
    • The new version of PC module is now compatible with Lab View 05/08/2014
    • A laptop PC can be ordered for $500 together with the furnace. We recommend ordering a computer (laptop) from us to avoid software installation problems as we will perform installation and testing before shipping. For more information please click here

Vacuum Flanges

  • SS water-cooled flanges on both sides. 
  • Left flange:
    1/4" thermocouple feedthrough
    1/4'' tube fitting
  • Right flange:
    KF 25 port with a right angle gate valve for vacuum pump
    Needle valve with barb fitting as a venting port
  • A digital vacuum gauge is included
  • Retractable bellow design is optional on the left flange, which allows sample flash heating or retrieving for fast cooling under inert gas. 

Vacuum Level

  •  Limited by the vacuum pump
    • 10^-2 torr can be achieved by the mechanical pump
    • 10^-4 torr can be reached by molecular pump
  • The pump is not included. ( please click the picture below to order )
  •  

Water Chiller (optional)

  • Cooling water is required for the flange set.
  • Please make sure the flow rate of cooling water is ≥ 10L/min, water temp. < 25ºC; pressure > 25 PSI.
  • We suggest EQ-KJ5000 Series recirculating water chiller as a cooling system (please order separately at related products below).

Laptop, software & WiFi Control (Optional)

  • Brand new laptop with Microsoft Windows 10 and Microsoft Office 2013 (30 days free trial) for immediate use.
  • Labview Based Temperature Control System (MTS01)enables the user to edit temperature profile, manage heat-treatment recipe, record and plot data for MTI furnaces.
  • A wireless remote control provides up to 300 meters of operating range.
  • The features above are available upon request at an extra cost (up to $1,000). Please contact us for more information.
  • Note: The software is only compatible with MTI’s Yudian Temperature Controller

Compliance

  • CE Certified
  • NRTL(UL61010) or CSA certification is available upon request at extra cost. ( please click marks below to learn details )

Application Notes

Click here to learn the installation of a gas regulator

  • Tube furnaces with quartz tubes are designed for use under vacuum and low pressure < 0.12 MPa (absolute pressure).
  • Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operationClick here to learn the installation of a gas regulator.
  • The flow rate for gasses should be limited to < 200 SCCM (or 200 ml/min) for reducing thermal shocks to the tube
  • Vacuum limit definition for all quartz tube furnaces: * Vacuum pressures may only be safely used up to 1000°C
  • Click here to learn how to set up a quartz/ ceramic tube and vacuum flange for MTI Tube furnace.
  • Quartz tubes should be replaced after every 10th use to ensure the best performance. 
  • Samples should never be placed on the tube directly; please order crucibles and boats from here.
  • After CVD, the graphene must be transferred from the metal catalyst to another substrate for most applications. By using the graphene transfer tape, the residue can below.

 

Dimension:

  • 1300mm(L) ×600mm(W) ×810mm(H)

Net Weight:

  • ~180 Kg

Shipping Weight:

  • 500 lbs



MTI offers a One-Year limited warranty for this product.

The MTI One Year Limited Warranty does NOT cover

  • Consumable parts, such as graphite dies, O-rings, crucibles, screws, washers, glassware, etc.
  • Any damage and rust resulting from improper storage or maintenance.
  • Any damages caused by the use of corrosive and acidic gases.
  • Any damage resulting from failing to adhere to the individual product's specific operation requirements, such as water cooling, venting, etc.
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