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32-Station (20g) Automatic Arc Melting System for High Throughput Alloy Research- SP-MSM360

32-Station (20g) Automatic Arc Melting System for High Throughput Alloy Research- SP-MSM360

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EQ-SP-MSM360 is a customized 32-station automatic Arc Melting System for high throughput MGI research such as alloy formation and phase diagram developments. Such an arc melting system consists of a gas-controlled/Vacuum glove box with CNC three-axis (X, Y, Z) of movement for precise "arc stinger" to "hearth cavity" positioning and stirring operations. Up to 32 alloy specimens (two 16-cavity copper crucibles) can be produced in a single batch in an ultra-clean environment (<1 ppm H2O and O2 level). Manual arc melting operation with a handheld arc melting stinger is also available. It is an efficient and economical system for high throughput MGI research of new-generation High-Entropy Alloys.

SPECIFICATIONS:

Features


  • Designed for high throughput, automatic arc melting of 32 samples (each sample weight <10g iron-based alloy) up to 3000 in a single batch (Various crucible design is available upon request)
  • Glove-box ensures arc melting in an ultra-clean gas environment with <1ppm H2O and O2 level
  • Water-cooled copper crucible, crucible grid cover, and vacuum dust removal (optional) allow arc melting of multiple samples without cross-contamination.
  • 4 mm diameter tungsten electrode is mounted on a CNC three-axis (X, Y, Z) stage inside the glove box. 
  • The tungsten electrode can be programmed with stirring motion for uniform arc melting of large samples.
  • A powerful arc melting power supply enables reliable, stable arc ignition.
  • Manual arc melting with a handheld stinger is available.
Structure
  • The high throughput, automatic arc melting system consists of 
    • Standard glove-box with <1ppm H2O and O2 purification system
    • Two 16-cavity copper crucibles (32 cavities total) with water cooling
    • Water-cooled tungsten electrode integrated with CNC three-axis (X, Y, Z) stage
    • Handheld arc melting stinger with KF40 feedthrough.
    • 16 L/min recirculating water chiller for cooling the copper crucibles and arc melting stinger.
Arc Melting & Copper Hearth

  

  
  • Metals are melted with an electric arc in a water-cooled copper crucible which has 32 cavities (25mm Dia x 8mm depth each). This allows the melting (up to 3000°C) of 32 specimens in a single batch without cross-contamination (see pic.1 and pic.2 below)
  • The Stainless steel crucible grid cover is included to protect the samples from cross-contamination ( pic.2) 
  • The vacuum vapor removal fixture is installed on the CNC stage to minimize cross-contamination during arc melting of low melting point materials. (see pic.3 below)
  • 4 mm diameter tungsten electrode /arc stinger is installed inside the glovebox with CNC X, Y, Z positioning (see pic.4 below). 
  • The water-cooled rectangular copper hearth is installed on the X (or Y) axes motion table.  
  •   pic.1    Pic. 2  Pic. 3    Pic. 4
CNC Positioning
  
  • Touch screen CNC three linear axes (X-Y-Z) of motion enables precise "arc stinger" to "hearth cavity" positioning as programmed to achieve automatic melting by touching one button.  
  • Arc stinger motion is driven by several step motors to achieve X, Y, Z or circle moment for the best melting result
  • The arc stinger travels in the pattern shown in the picture on the left.
  • The stirring motion of the arc melting stinger can be programmed for the uniform melting of large samples.
  • For each sample, the arc melting operation consists of two steps: stationary arcing step and stirring step (1 - 10mm diameter adjustable stirring motion)
  • X, Y, Z motion speed: ≤ 800mm/min
Gas-Controlled Glove Box
        
  • Glove Box: EQ-VGB-6OP-LD (see pic.1 below)
  • Operation Environment: dry environment with good ventilation, 15-25 . Air conditioner (not included) is required if out of this range.
  • Glove-box chamber dimension: 1200mm x 740mm x 900mm (LxWxH)
  • Two airlock chambers:
    • Large antechamber dimension: 360mm ID x 600mm L
    • Small antechamber dimension: 150mm ID x 220mm L
  • Two 175mm diameter glove ports with a pair of 8" Butadyl gloves.
  • Filter system: gas outlet filters can eliminate particle size > 0.3μm
  • Openable front window panel for easy equipment loading
  • Arc melting stinger/gun with KF40 feedthrough to connect into the glovebox (see pic.2 and pic.3 below)
  • Glove Box with H2O & O2 Purification System and Openable Front Window is included with all necessary feedthrough, which includes CNC stage control cable, cooling water inlet & outlet, arc melting power +/-, handheld arc melting stinger, and vacuum dust removal. (see pic.4 below)
       pic.1      pic.2  pic.3    pic.4
Arc Melting Power Supply  

  • Input Voltage: 110 or 220 VAC selectable, single phase  
  • Current: 34 A max (40A circuit breaker integrated). Recommend power source breaker ≥ 40A
  • Rated DC output: 
    • 15V/ 125A at 35% duty cycle - 110V input
    • 18V/ 185A at 35% duty cycle - 220V input
  • Minimum DC current output: 5A
  • Pulse DC and AC output modes are available.
Gas Purification System 
  • Automatic moisture and oxygen removal to <1 ppm (20, 1 atm)
  • Pressure Range: ± 12m-bar
  • 240 L/m Heavy-duty mechanical vacuum pump with exhaust filter is included. 
  • Precision Humidity Analyzer with KF25 Flange (0-999 ppm) and the oxygen sensor is installed on the Purification System with an accuracy of +/- 0.1 ppm
  • Large capacity moisture filter built in the bottom of the mobile cart, which can absorb moisture up to 1.5 kg
  • The regeneration Temperature Controller is built-in for filter regeneration
  • An automatic pressure control system can keep the pressure at a constant level. Manual pressure control is allowed via a foot pedal.
  • The touch screen panel enables easy setting, humidity, oxygen concentration, and pressure level display
  • The removable control panel can be placed on the side for easy operation
Water Chiller & Gas
    
  • MTI's KJ-5000 recirculating water chiller (16 L/min) is included for the water cooling of copper crucibles and arc melting stinger.
  • High-purity Argon gas is with at least 5N purity (>99.999%) required (not included) for the arc melting process.  
  • 5% Hydrogen + 95% Argon gas is needed for regenerating the purification station (not included)
Dimensions System dimension: 2300mm x 1230mm x 1880mm (LxWxH)
Shipping Weight & Dimensions
  • Two Pallets
  • #1: 1455 lbs, 80"x41"x87"
  • #2: 460 lbs, 48"x40"x30"
Warranty
  • One-year limited warranty with lifetime support
  • Rusting and damage due to improper storage conditions or maintenance are not covered by a warranty
  • Gloves and oxygen sensors are consumable parts that are NOT covered by warranty.
Compliance
  • CE certified
  • NRTL or CSA (UL 6101 ) Certification is available upon request at additional charges    
Application Notes & Warnings
  • Regularly perform regeneration to maintain optimum purification efficiency.
  • The O2 sensor is consumable and its expected lifespan is around one year. Please order an O2 sensor replacement at MTI
Manufacturer Part Number: