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1.7MHz Ultrasonic Spray Pyrolysis Furnace 1200C Max. for Synthesis Nanoparticles - OTF-1200X-PGEP

1.7MHz Ultrasonic Spray Pyrolysis Furnace 1200C Max. for Synthesis Nanoparticles - OTF-1200X-PGEP

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SKU: : \OTF-1200X-PGEP

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OTF-1200X-PGEP is a versatile ultrasonic spray furnace system designed for the synthesis of core-shell nanoparticles. Three major subsystems (ultrasonic enhanced aerosol generator, tube furnace, and electrostatic precipitator) are employed on three processes including aerosol generation, thermal decomposition, and nanoparticle collection. Such a system enables advanced synthetic method that provides control over particle size, morphology, and nano/microstructure.
   SPECIFICATIONS
System Features


  • Aerosol Generation: 1.7MHz Ultrasonic Enhanced Bubbler can "evaporate" target solution with literally no heat generated. An elongated Tee tube wrapped by a heating tape that connects inline with an ultrasonic bubbler can prevent condensing liquid from streaming into the tube furnace and promote the generation of aerosol. 
  • Thermal Decomposition: The tube Furnace can be heated up to 1200C maximum. By passing the aerosol flux across the temperature and flow rate-regulated firing zone, chemical and physical processes may proceed.  
  • Nanopowder Collection: an electrostatic precipitator (1.2 L, up to 30 kV) can effectively collect nanoparticles from the carrier gas flow
Tube Furnace -
Thermal Decomposition



Voltage & Power
  • Single Phase, 208V~240V AC, 50/60 Hz   (30A breaker required)
  • Max. 3 kW
Working Temperature
  • 1100°C  continuous
  • 1200°C  Max. < 1 hour
Max. Heating / Cooling Rate
  • < 20 °C / min 

Heating Zone & 
Temperature Uniformity
  • 12" total heating zone length
  • 3" ( ± 1 °C )  heating area with the best thermal uniformity.
Heating Elements
  • Fe-Cr-Al Alloy doped by Mo
Temperature Controller

  • PID automatic control, 30 programmable segments for precise control of heating rate, cooling rate, and dwell time.
  • Built-in over-temperature alarm and protection allow for operation without the attendant.
  • ± 1 ºC temperature control at dwelling process
  • RS485 Communication Port.
Processing Tube
  • The high-quality fused quartz tube is included for operation @ 1200C.
  • (I.D.: 21mm x OD: 25mm x 1200 mm length). 
Flanges & Fittings
  • Left flange: KF25 quick-connect
  • Right flange: KF25 quick-connect
Aerosol Generation

Ultrasonic Generator


  • 316 Stainless Steel liquid container equipped with a fluoropolymer sealing ring and a heating tape
  •  1.7 MHz ultrasonic generator installed with a PEEK base
  • 3 levels of power output ( low = "1", liquid injection speed = 0.2 mL/min), (middle = "2", liquid injection speed = 0.4 mL/min),  (high ="3", liquid injection speed = 0.6 mL/min). To achieve high atomizing quality, the syringe pump rate should be match with the power output level. 
  • 7 levels of time setting ("Out" indicator light), "1" =  no limited timing, "2" = 30 min, "3"= 60 min, "4"= 90 min, "5"= 120 min, "6"= 150 min, "7" = 180 min   
  • Droplet size: < 10 microns, which is dependent on the viscosity of the solution, ultrasonic frequency, and gas speed.
  • Continuous mode and timed mode can be set. 
  • The quick clamps allow easy removal of components for cleaning or adapting the device with simple connections to the gas supply
Digital Syringe Pump
  • Holds small or big syringes up to 60 mL
  • Pumps continuously until you stop the pump
  • The infusion rate can be changed while pumping
  • Remembers previous settings on power-up
  • Power failure mode allows the pump to continue pumping after a reset
  • The maximum pumping rate of 25 mL/min with a 60 mL syringe
  • Selectable infusion rates units: mL/hr, µL/hr, mL/min, µL/min
  • Infuses Only does not withdraw, volume target, or have a computer interface
  • An infusion Syringe Pump with an optional Heatable Glass Syringe is available at an extra cost
Flow Meter

  • A 0-1000 ml/min floating flow meter is included to control the carrier gas flow rate.
  • The mass flow meter is optional at an extra cost. (EQ-MFC-GFC-LD)
Nanopowder Collection
  • 24VDC input high voltage power supply up to 30KV, 30 W Max. power consumption
  • Digital Voltmeter and Current meter
  • Output voltage and current can be set by using knobs on the front panel and read from the digital display
  • Constant current/Constant Voltage mode of operation
  • Built-in Arc Protection Circuit
Electrostatic Precipitator

   
  • Up to 30 kV and 1 mA.
  • A KF25 quick clamp and flange enables the quick coupling to the furnace processing tube.
  • Another KF25 port is built-in with the collector to connect the vacuum pump (The vacuum pump is required, but it is not included in the standard package.)
  • PTFE plates are installed on top and bottom to insulate high-voltage electrodes
  • 12mm gas outlet built-in.
  • The electrode rod is in the shape of a cross, increasing surface area compared to cylindrical electrodes.
  • Adjustable supports keep the collector leveled with the furnace tub.
  • Double layer design, please check the picture shown on the left.
  • Net Weight
  • 180Kg
Overall Dimension  (Click the pic for more detail)
Shipping Dimension & Weight
  • 48"x40"x62"
  • 500 lbs
Warranty
  • One-year limited manufacturer warranty with lifetime support (consumable parts such as furnace liner, processing tubes, and O-rings are not covered by the warranty, please order replacements for related products below).
Laptop, software & WiFi Control (Optional)
    
Manufacturer Part Number: